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| 制备高纯度雷酸金的工艺研究 |
| Preparation of Highly Purified Fulminating Gold |
| Received:August 20, 2013 |
| DOI： |
| 中文关键词: 无机化学 雷酸金 金含量 洗涤水 洗涤处理 |
| 英文关键词: inorganic chemistry fulminating gold gold content distilled water distilled water setting |
| 基金项目: |
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| 中文摘要: |
| 在旋转蒸发体系中，研究雷酸金的制备方法，并探索了不同条件下雷酸金产品的金含量。实验结果表明在105℃下蒸发45 min为相对最优制备条件；用90℃蒸馏水洗涤90 min为雷酸金最佳后续处理条件。 |
| 英文摘要: |
| The method of preparing fulminating gold was studied in a rotary evaporator. The different conditions were explored to correlate with the gold content of final products. Experimental results show that the optimum setting of preparing fulminating gold is evaporation at 105℃ for 45 min; the optimum setting for subsequent processing is rinsing fulminating gold for 90 min with distilled water of 90℃. |
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