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| 制备高活性二氯四氨合钯(II)的工艺研究 |
| Preparation of Highly Activity Tetraamminepalladium(II) Chloride |
| Received:July 07, 2014 |
| DOI： |
| 中文关键词: 无机化学；二氯四氨合钯(II)；制备 钯含量；重结晶 |
| 英文关键词: inorganic chemistry tetraamminepalladium(II) chloride preparing palladium content recrystallization |
| 基金项目: |
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| 中文摘要: |
| 在旋转蒸发仪中，研究了二氯四氨合钯(II)的制备方法，并探索了不同反应条件下二氯四氨合钯(II)产品的钯含量。结果表明，四氯合钯酸在85℃下与氨水反应80 min为相对最优制备条件；在70℃下重结晶25 min为二氯四氨合钯(II)最佳后续处理条件。 |
| 英文摘要: |
| The method of preparing tetraamminepalladium(II) chloride was studied in a rotary evaporator. The different conditions were explored to correlate with the palladium content of final products. Experimental results show that the optimum setting of preparing tetrachloropalladate acid is reaction with ammonia at 85℃ for 80 min; the optimum setting for subsequent processing is recrystallization at 70℃ for 25 min. |
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