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| 硫酸加压溶解法从氧化铝基废催化剂中回收铂 |
| Recovering Platinum from Alumina-based Spent Catalysts by Sulfuric Acid Pressure Dissolution |
| Received:July 29, 2015 |
| DOI： |
| 中文关键词: 有色金属冶金 废催化剂 加压 硫酸 铂 回收 |
| 英文关键词: nonferrous metallurgy spent catalyst pressure sulfuric acid platinum recovery |
| 基金项目:云南省省院省校科技合作项目(2013IB020) |
| Author Name | Affiliation | | ZHAO Yu | Sino-Platinum Metals Resources Yimen Co. Ltd., Sino-Platinum Metals Co. Ltd., State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metals, Kunming 650106, China | | WANG Huan | Sino-Platinum Metals Resources Yimen Co. Ltd., Sino-Platinum Metals Co. Ltd., State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metals, Kunming 650106, China | | HE Xiaotang | Sino-Platinum Metals Resources Yimen Co. Ltd., Sino-Platinum Metals Co. Ltd., State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metals, Kunming 650106, China | | GUO Junmei | Sino-Platinum Metals Resources Yimen Co. Ltd., Sino-Platinum Metals Co. Ltd., State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metals, Kunming 650106, China | | HAN Shouli | Sino-Platinum Metals Resources Yimen Co. Ltd., Sino-Platinum Metals Co. Ltd., State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metals, Kunming 650106, China | | WU Xilong | Sino-Platinum Metals Resources Yimen Co. Ltd., Sino-Platinum Metals Co. Ltd., State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metals, Kunming 650106, China | | LI Yong | Sino-Platinum Metals Resources Yimen Co. Ltd., Sino-Platinum Metals Co. Ltd., State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metals, Kunming 650106, China | | LI Hongmei | Sino-Platinum Metals Resources Yimen Co. Ltd., Sino-Platinum Metals Co. Ltd., State Key Laboratory of Advanced Technologies for Comprehensive Utilization of Platinum Metals, Kunming 650106, China |
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| 中文摘要: |
| 研究了硫酸加压溶解法从氧化铝基含铂废催化剂中回收铂。在高压釜中，反应温度130℃，压力4.5 kg/cm2，时间4 h，氧化铝载体的溶解效率较好；添加TiCl3溶液可将分散到溶液中的铂浓度降低至0.0005 g/L以下；富集物经溶解-精炼得到纯度大于99.98%的海绵铂，铂直收率为98.71%。 |
| 英文摘要: |
| A method of sulfuric acid pressure dissolution to recover platinum from the waste alumina-based catalysts was studied. The selective dissolution was carried out in the autoclave for 4 h at a temperature of 130℃ and under pressure of 4.5 kg/cm2, producing a desired result. Platinum dissolved in the solution could be reduced to a concentration of less than 0.0005 g/L by adding TiCl3 as a reductant. Sponge platinum with a purity of 99.98% was obtained from insoluble substance after the melting-refining process, and the direct recovery of platinum was up to 98.71%. |
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