Abstract
等离子熔炼富集物Fe-PGM合金的取样方法研究
Study on Sample Preparation and Sampling Method for Analysis of Plasma Smelting Fe-PGM Alloy
Received:September 24, 2015  
DOI:
中文关键词: 分析化学  Fe-PGM合金  取样  制样
英文关键词: analytical chemistry  plasma smelting  Fe-PGM alloy  sampling  preparation
基金项目:稀贵金属综合利用新技术国家重点实验室项目(SKL-SPM-201541)。
Author NameAffiliationE-mail
LIU Wei Sino-Platinum Metals Resources Yimen Co. Ltd., State Key Laboratory Advanced Technologies forComprehensive Utilization of Platinum Metals, Sino-Platinum Metals Co. Ltd., Kunming 650106, China liuweiynkm@sina.com 
LI Yong Sino-Platinum Metals Resources Yimen Co. Ltd., State Key Laboratory Advanced Technologies forComprehensive Utilization of Platinum Metals, Sino-Platinum Metals Co. Ltd., Kunming 650106, China  
LIU Wen Sino-Platinum Metals Resources Yimen Co. Ltd., State Key Laboratory Advanced Technologies forComprehensive Utilization of Platinum Metals, Sino-Platinum Metals Co. Ltd., Kunming 650106, China  
JIN Yunjie Sino-Platinum Metals Resources Yimen Co. Ltd., State Key Laboratory Advanced Technologies forComprehensive Utilization of Platinum Metals, Sino-Platinum Metals Co. Ltd., Kunming 650106, China  
LIN Bo Sino-Platinum Metals Resources Yimen Co. Ltd., State Key Laboratory Advanced Technologies forComprehensive Utilization of Platinum Metals, Sino-Platinum Metals Co. Ltd., Kunming 650106, China  
LUO Xian Sino-Platinum Metals Resources Yimen Co. Ltd., State Key Laboratory Advanced Technologies forComprehensive Utilization of Platinum Metals, Sino-Platinum Metals Co. Ltd., Kunming 650106, China  
SONG Zenkai Sino-Platinum Metals Resources Yimen Co. Ltd., State Key Laboratory Advanced Technologies forComprehensive Utilization of Platinum Metals, Sino-Platinum Metals Co. Ltd., Kunming 650106, China  
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中文摘要:
      对等离子熔炼Fe-PGM合金物料的取制样方法进行了研究。物料经破碎至40目,混匀,均分为12个网格,每个网格钎取20 g样品,混合得到240 g大样,大样进一步研磨至150目得到分析样品。经物料均匀性检验和取样代表性分析,表明取样方法可满足物料取样和分析要求。
英文摘要:
      A sample preparation and sampling method for analysis of plasma smelting Fe-PGM alloy was studied. The alloy was crushed to 40 mesh size, homogeneously mixed, divided into 12 grids. From every grid, a sample of 20 g was taken, and then mixed together to produce a large sample weighing 240 g which was subjected to the fine grind process to give an analytical sample. Homogeneity and representativeness tests show that the sampling method meets the analytical requirements for Fe-PGM alloy.
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