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| 含银废电子浆料中银的浸出和除杂工艺条件研究 |
| Conditions of Leaching and Purifying Process for Recycling Silver from Waste Silver-Bearing Electronic Paste |
| Received:November 13, 2015 |
| DOI： |
| 中文关键词: 银 浸出 除杂 含银废电子浆料 |
| 英文关键词: silver leaching purifying waste silver-bearing electronic paste |
| 基金项目:国家科技支撑计划项目(项目号2014BAC03B06，废旧电子元器件中稀贵金属和热塑性塑料高值化清洁利用关键技术及示范)；江苏省科技支撑计划项目(项目号BE2012645，废电路板器分离与高值资源选择性富集技术研究)。 |
| Author Name | Affiliation | E-mail | | WANG Lingling | Jiangsu University of Technology, Changzhou 213001, Jiangsu, China | silence0609@foxmail.com | | CHEN Chen | Jiangsu University of Technology, Changzhou 213001, Jiangsu, China | | | ZHU Binglong | Jiangsu University of Technology, Changzhou 213001, Jiangsu, China | | | TONG Fei | Jiangsu University of Technology, Changzhou 213001, Jiangsu, China | | | ZHOU Quanfa | Jiangsu University of Technology, Changzhou 213001, Jiangsu, China | labzqf@jsut.edu.cn |
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| 中文摘要: |
| 用硝酸作为浸出剂，通过正交试验考察了各工艺条件对含银电子废料中的银的浸出效率的影响。结果表明，硝酸浓度和浸出温度是影响浸出效率的主要因素；在硝酸浓度为8 mol/L、搅拌速度为100 r/min、浸出温度和时间分别为80℃和80 min的最佳条件下，浸出效率可达88%以上。控制温度为70℃，以NaOH溶液调节浸出液至近中性(pH=6.0)，共存杂质Cu、Fe、Pb、Ni和Bi的一次去除率达到80%以上，可得到较纯净的硝酸银溶液。 |
| 英文摘要: |
| Theleaching rate of silver from the waste silver-bearing electronic paste using nitric acid as the leaching agent was investigated by the orthogonal test. Experimental results show that the concentration of nitric acid and leaching temperature are the main factors affecting the leaching rate. A high leaching rate of 88% was realized when the leaching was carried out in 8 mol/L nitric acid solution for 80 min at 80℃ with a stirring speed of 100 rpm. More than 80% of Cu, Fe, Pb, Ni and Bi ions co-existing in the lixivium could be removed at 70℃ by adjusting the pH value of the lixivium to 6. |
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