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| 分子识别技术分离提纯钯的工艺实验 |
| Experimental study on the separation and purification of palladium by molecular recognition technology |
| Received:July 15, 2021 |
| DOI： |
| 中文关键词: 冶金技术 分子识别技术 铂钯分离 钯精炼 |
| 英文关键词: metallurgical technology molecular recognition technology separation of platinum and palladium palladium refining |
| 基金项目:云南省科技人才和平台计划项目(2018HB112)；固废资源化专项(2019YFC1907505) |
| Author Name | Affiliation | E-mail | | WU Xi-long | Sino-Platinum Metals Resources Yimen Co. Ltd., Yuxi 651100, Yunnan, China | 291283488@qq.com | | HE Xiao-tang | Sino-Platinum Metals Resources Yimen Co. Ltd., Yuxi 651100, Yunnan, China | | | LI Yong | Sino-Platinum Metals Resources Yimen Co. Ltd., Yuxi 651100, Yunnan, China | | | ZHAO Yu | Sino-Platinum Metals Resources Yimen Co. Ltd., Yuxi 651100, Yunnan, China | | | WANG Huan | Sino-Platinum Metals Resources Yimen Co. Ltd., Yuxi 651100, Yunnan, China | |
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| 中文摘要: |
| 采用分子识别材料SuperLigò2从含铂钯的溶液中选择性分离钯，钯吸附率大于99%，吸附、洗脱过程钯的直收率为95.87%，总收率为98.04%；得到的洗脱液氧化处理后生成钯沉淀，再经水合肼还原即可得到纯度为99.99%的钯粉。与传统的沉淀分离工艺相比，分子识别技术的生产流程短、铂不容易分散、操作方便、三废量少。 |
| 英文摘要: |
| The molecular recognition material SuperLigò2 was used to selectively separate palladium from the solution containing platinum and palladium. The adsorption rate of palladium was more than 99%, and the direct yield of palladium was 95.87%, and the total yield was 98.04%. The obtained palladium eluent was oxidized to obtain palladium precipitation, which is then reduced by hydrazine hydrate to obtain palladium powder with a purity of 99.99%. Compared with the traditional precipitation separation process, the molecular recognition technology has a shorter production process, less platinum dispersion, convenient operation and less waste. |
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