Abstract
高温涂层包覆贵金属热电偶的性能研究
Study on properties of precious metal thermocouples coated with high temperature-resisting wear
Received:March 04, 2022  
DOI:
中文关键词: 等离子喷涂  高温涂层  贵金属热电偶  稳定性
英文关键词: plasma spraying  high temperature coating  precious metal thermocouple  stability
基金项目:国家自然科学基金(U20A20232)
Author NameAffiliation
LI Feng Chongqing Materials Research Institute Co.Ltd., National Instrument Functional Materials Engineering TechnologyResearch Centers, Chongqing 400707 
TANG Hui-yi Chongqing Materials Research Institute Co.Ltd., National Instrument Functional Materials Engineering TechnologyResearch Centers, Chongqing 400707 
XIAO Yu-chen Chongqing Materials Research Institute Co.Ltd., National Instrument Functional Materials Engineering TechnologyResearch Centers, Chongqing 400707 
WU Bao-an Chongqing Materials Research Institute Co.Ltd., National Instrument Functional Materials Engineering TechnologyResearch Centers, Chongqing 400707 
YANG Kai-zhou Chongqing Hangli Industrial Co.Ltd., Chongqing 401346 
ZHENG Ya-wen Chongqing Materials Research Institute Co.Ltd., National Instrument Functional Materials Engineering TechnologyResearch Centers, Chongqing 400707 
SUN Lin Chongqing Materials Research Institute Co.Ltd., National Instrument Functional Materials Engineering TechnologyResearch Centers, Chongqing 400707 
ZHENG Lei Chongqing Materials Research Institute Co.Ltd., National Instrument Functional Materials Engineering TechnologyResearch Centers, Chongqing 400707 
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中文摘要:
      通过等离子喷涂方法,使高温涂层均匀包覆在贵金属热电偶(Pt-10Rh/Pt)的裸丝上,其涂层厚度为30~50 μm,并对样品进行稳定性试验。采用金相显微镜及扫描电镜对样品稳定性试验前后的涂层形貌、厚度、均匀性进行观察,结果表明:高温包覆涂层在贵金属裸丝上致密、均匀的分布,其长期稳定性比裸丝更好。样品在经过1400℃/200 h保温后,裸丝晶粒粗大,而高温涂层包覆的丝材晶粒比裸丝晶粒细小,高温涂层对贵金属丝材起到了一定的保护作用,增加贵金属偶丝的使用寿命,降低使用成本。
英文摘要:
      The plasma spraying method was chosen in our study to make the high temperature-resisting coating on the bare wire of precious metal thermocouple(Pt-10Rh/Pt), and the coating thickness was 30~50 μm. Then the stability test of the sample was conducted. Metallographic microscope and scanning electron microscope were used to observe the coating morphology, thickness and uniformity before and after the stability test. The results showed that the coating was densely and uniformly distributed on the precious metal bare wires, and the stability was improved. The grain size of the wires with the coating was much smaller than that of the bare wires after the test at 1400℃ for 200 h. Therefore, the high temperature-resisting coating can protect precious metal base wires, increase their service life and reduce the cost.
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